An Investigation on Synthesis of Silver Nanoparticles

Md. Ashraful Alam

Institute of Glass and Ceramic Research and Testing (IGCRT), Bangladesh Councill of Scientific and Industrial Research (BCSIR), Dhaka-1205, Bangladesh.

Salma Akter Munni

Institute of Glass and Ceramic Research and Testing (IGCRT), Bangladesh Councill of Scientific and Industrial Research (BCSIR), Dhaka-1205, Bangladesh.

Sabrina Mostafa

Institute of Glass and Ceramic Research and Testing (IGCRT), Bangladesh Councill of Scientific and Industrial Research (BCSIR), Dhaka-1205, Bangladesh.

Raton Kumar Bishwas

Institute of Glass and Ceramic Research and Testing (IGCRT), Bangladesh Councill of Scientific and Industrial Research (BCSIR), Dhaka-1205, Bangladesh.

Shirin Akter Jahan *

Institute of Glass and Ceramic Research and Testing (IGCRT), Bangladesh Councill of Scientific and Industrial Research (BCSIR), Dhaka-1205, Bangladesh.

*Author to whom correspondence should be addressed.


Abstract

Introduction: Nano science and nano biotechnology provided enormous opportunities for exploring the bactericidal and fungicidal activities. Since ancient times, silver was known for its anti-bacterial effects and for centuries it has been used for prevention and control of disparate infections. On the effective use silver nanomaterials synthesized and characterized play a vital role of the modern science.

Aims: Our goal is to prepare silver nanomaterials since studies have shown that silver nanoparticles have efficient activity against bacterial biofilms.

Methodology: The silver nanoparticles were generally synthesized by non-aqueous sol-gel technique in the presence of different precursor by chelating agent.

Results: Here found a cubic unit cell with miller indices (111) (200) (220) (311) (222) and crystallite size around 50.00nm by XRD. The morphology of the prepared nano particles has been revealed by SEM below 10.00 nm and TEM is below 5.00nm in size of graphical presentation such as size, shape, surface etc. of the nanoparticles. DLS is a unique technique to discern particle size around 65.00nm and size distributions in aqueous or physiological solutions of the nanoparticles.

Conclusion: The studies on the combined synthesized and use of AgNPs with other antimicrobial agents generally help reduce the problem of toxicity and to avoid the potential for development of resistance and strongly enhance the microbicidal effect. This paper describes a short and very precise description about the chemical synthesis process of silver nanoparticles like no aqueous SGM. Also, this paper contains a brief description about different characterization technique of nanoparticles like X-ray Diffraction review the shape of crystal a cubic unit cell with miller indices (111) (200) (220) (311) (222) where crystallite size around 50.00nm, the morphology of the prepared nanoparticles has been revealed with size 10.00nm by SEM, Dynamic Light Scattering discern particle size around 65.00nm and Transmission Electron Microscope review the spherical shape of the nanomaterials.  Further investigation will be continuing the antimicrobial activity test of AgNPs with ceramic coating.

Keywords: Cell destruction (CD), silver nanoparticles (AgNPs), sol-gel method (SGM), TEM analysis (TA), XRD technique (XRDT)


How to Cite

Alam , M. A., Munni , S. A., Mostafa , S., Bishwas , R. K., & Jahan , S. A. (2023). An Investigation on Synthesis of Silver Nanoparticles. Asian Journal of Research in Biochemistry, 12(3), 1–10. https://doi.org/10.9734/ajrb/2023/v12i3234

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